Crystallography Open Database

Information card for entry 4302969

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Coordinates	4302969.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H88 As8 Na6 O56 Pd13
Calculated formula	C48 H40 As8 O64 Pd13
Title of publication	Heteropoly-13-Palladates(II) [PdII13(AsVPh)8O32]6- and [PdII13SeIV8O32]6-
Authors of publication	Natalya V. Izarova; Michael H. Dickman; Rosa Ngo Biboum; Bineta Keita; Louis Nadjo; Vasanth Ramachandran; Naresh S. Dalal; Ulrich Kortz
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	7504 - 7506
a	15.9515 ± 0.0008 Å
b	15.9515 ± 0.0008 Å
c	25.1154 ± 0.0012 Å
α	90°
β	90°
γ	90°
Cell volume	6390.6 ± 0.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	87
Hermann-Mauguin space group symbol	I 4/m
Hall space group symbol	-I 4
Residual factor for all reflections	0.099
Residual factor for significantly intense reflections	0.051
Weighted residual factors for significantly intense reflections	0.1384
Weighted residual factors for all reflections included in the refinement	0.1656
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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