Information card for entry 4302970

Structure parameters

• Formula: C48 H74 As8 K3 N0 Na3 O49 Pd13
• Calculated formula: C48 H30 As8 K3 Na3 O49 Pd13
• Title of publication: Heteropoly-13-Palladates(II) [PdII13(AsVPh)8O32]6- and [PdII13SeIV8O32]6-
• Authors of publication: Natalya V. Izarova; Michael H. Dickman; Rosa Ngo Biboum; Bineta Keita; Louis Nadjo; Vasanth Ramachandran; Naresh S. Dalal; Ulrich Kortz
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 7504 - 7506
• a: 13.4351 ± 0.0005 Å
• b: 14.3952 ± 0.0005 Å
• c: 14.8476 ± 0.0004 Å
• α: 97.357 ± 0.002°
• β: 107.626 ± 0.002°
• γ: 103.969 ± 0.002°
• Cell volume: 2592.22 ± 0.16 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0766
• Residual factor for significantly intense reflections: 0.0462
• Weighted residual factors for significantly intense reflections: 0.1279
• Weighted residual factors for all reflections included in the refinement: 0.1479
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No