Crystallography Open Database

Information card for entry 4302981

Preview

Coordinates	4302981.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C91.5 H80 Cl6 Fe4 O4 P4
Calculated formula	C91.5 H80 Cl6 Fe4 O4 P4
Title of publication	Synthesis of Binuclear Complexes Bound in an Enlarged Tetraphosphamacrocycle: Two Diphosphine Metal Units Linked in Front-to-Front Style
Authors of publication	Tsutomu Mizuta; Yuta Inami; Kazuyuki Kubo; Katsuhiko Miyoshi
Journal of publication	Inorganic Chemistry
Year of publication	2009
Journal volume	48
Pages of publication	7534 - 7536
a	16.898 ± 0.0004 Å
b	17.274 ± 0.0004 Å
c	17.38 ± 0.0005 Å
α	69.996 ± 0.001°
β	69.621 ± 0.001°
γ	62.037 ± 0.001°
Cell volume	4101.29 ± 0.18 Å³
Cell temperature	200 ± 2 K
Ambient diffraction temperature	200 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1249
Residual factor for significantly intense reflections	0.0707
Weighted residual factors for significantly intense reflections	0.1572
Weighted residual factors for all reflections included in the refinement	0.1905
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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