Information card for entry 4302982

Structure parameters

• Formula: C82 H78 Ag2 B2 F8 Fe4 N6 O4 P4
• Calculated formula: C82 H78 Ag2 B2 F8 Fe4 N6 O4 P4
• Title of publication: Synthesis of Binuclear Complexes Bound in an Enlarged Tetraphosphamacrocycle: Two Diphosphine Metal Units Linked in Front-to-Front Style
• Authors of publication: Tsutomu Mizuta; Yuta Inami; Kazuyuki Kubo; Katsuhiko Miyoshi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 7534 - 7536
• a: 32.233 ± 0.0004 Å
• b: 32.233 Å
• c: 47.969 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 43161.1 ± 0.8 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 9
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0885
• Residual factor for significantly intense reflections: 0.0708
• Weighted residual factors for significantly intense reflections: 0.1762
• Weighted residual factors for all reflections included in the refinement: 0.188
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No