Information card for entry 4303388

Structure parameters

• Formula: C48 H70 I N4 O Si2 Yb
• Calculated formula: C48 H70 I N4 O Si2 Yb
• SMILES: [Yb]12(I)([O]5CCCC5)([N](c5c(cccc5C(C)C)C(C)C)=C(N1[Si](C)(C)C)c1ccccc1)[N](c1c(cccc1C(C)C)C(C)C)=C(N2[Si](C)(C)C)c1ccccc1
• Title of publication: Synthesis, Structure, and Reaction Chemistry of Samarium(II), Europium(II), and Ytterbium(II) Complexes of the Unsymmetrical Benzamidinate Ligand [PhC(NSiMe3)(NC6H3Pri2-2,6)]-
• Authors of publication: Shuang Yao; Hoi-Shan Chan; Chi-Keung Lam; Hung Kay Lee
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 9936 - 9946
• a: 14.241 ± 0.002 Å
• b: 14.095 ± 0.002 Å
• c: 25.946 ± 0.004 Å
• α: 90°
• β: 95.391 ± 0.002°
• γ: 90°
• Cell volume: 5185 ± 1.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0466
• Residual factor for significantly intense reflections: 0.0315
• Weighted residual factors for significantly intense reflections: 0.075
• Weighted residual factors for all reflections included in the refinement: 0.084
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No