Information card for entry 4303389

Structure parameters

• Formula: C57 H85 N6 Si2 Sm
• Calculated formula: C57 H85 N6 Si2 Sm
• SMILES: c1(c(cccc1C(C)C)C(C)C)[N]1=C(N([Si](C)(C)C)[Sm]231([N](=CN2C1CCCCC1)C1CCCCC1)[N](c1c(cccc1C(C)C)C(C)C)=C(N3[Si](C)(C)C)c1ccccc1)c1ccccc1
• Title of publication: Synthesis, Structure, and Reaction Chemistry of Samarium(II), Europium(II), and Ytterbium(II) Complexes of the Unsymmetrical Benzamidinate Ligand [PhC(NSiMe3)(NC6H3Pri2-2,6)]-
• Authors of publication: Shuang Yao; Hoi-Shan Chan; Chi-Keung Lam; Hung Kay Lee
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 9936 - 9946
• a: 14.513 ± 0.003 Å
• b: 18.376 ± 0.003 Å
• c: 22.516 ± 0.004 Å
• α: 90°
• β: 102.796 ± 0.003°
• γ: 90°
• Cell volume: 5855.7 ± 1.9 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.052
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.0909
• Weighted residual factors for all reflections included in the refinement: 0.0993
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No