Information card for entry 4303912

Structure parameters

• Formula: C306 H296 B16 Co8 F64 N90 O37
• Calculated formula: C306 H294 B14 Co8 F56 N90 O37
• Title of publication: Cubes, Squares, and Books: A Simple Transition Metal/Bridging Ligand Combination Can Lead to a Surprising Range of Structural Types with the Same Metal/Ligand Proportions
• Authors of publication: Adel M. Najar; Ian S. Tidmarsh; Harry Adams; Michael D. Ward
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 11871 - 11881
• a: 22.87 ± 0.003 Å
• b: 23.585 ± 0.003 Å
• c: 25.043 ± 0.003 Å
• α: 113.727 ± 0.006°
• β: 109.603 ± 0.007°
• γ: 101.195 ± 0.006°
• Cell volume: 10768 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1532
• Residual factor for significantly intense reflections: 0.1153
• Weighted residual factors for significantly intense reflections: 0.3283
• Weighted residual factors for all reflections included in the refinement: 0.3556
• Goodness-of-fit parameter for all reflections included in the refinement: 1.26
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No