Information card for entry 4303913

Structure parameters

• Formula: C276 H228 B16 Co8 F64 N84
• Calculated formula: C276 H228 B16 Co8 F64 N84
• Title of publication: Cubes, Squares, and Books: A Simple Transition Metal/Bridging Ligand Combination Can Lead to a Surprising Range of Structural Types with the Same Metal/Ligand Proportions
• Authors of publication: Adel M. Najar; Ian S. Tidmarsh; Harry Adams; Michael D. Ward
• Journal of publication: Inorganic Chemistry
• Year of publication: 2009
• Journal volume: 48
• Pages of publication: 11871 - 11881
• a: 19.59 ± 0.0009 Å
• b: 42.658 ± 0.002 Å
• c: 21.1943 ± 0.0009 Å
• α: 90°
• β: 113.099 ± 0.002°
• γ: 90°
• Cell volume: 16291.5 ± 1.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1321
• Residual factor for significantly intense reflections: 0.0985
• Weighted residual factors for significantly intense reflections: 0.2674
• Weighted residual factors for all reflections included in the refinement: 0.2897
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No