Information card for entry 4304800

Structure parameters

• Formula: C189 H184 Ge4 Ni2 P4 S8
• Calculated formula: C189 H160 Ge4 Ni2 P4 S8
• Title of publication: Synthesis of Ge2NiS4 Clusters and the Thermal Transformation to a Ge4Ni6S12 Cluster
• Authors of publication: Tsuyoshi Matsumoto; Yosuke Matsui; Mikinao Ito; Kazuyuki Tatsumi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 1901 - 1903
• a: 14.0364 ± 0.0014 Å
• b: 18.01 ± 0.003 Å
• c: 18.085 ± 0.003 Å
• α: 106.91 ± 0.006°
• β: 107.717 ± 0.0013°
• γ: 95.117 ± 0.002°
• Cell volume: 4086.7 ± 1.1 ų
• Cell temperature: 173.1 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0711
• Weighted residual factors for all reflections included in the refinement: 0.205
• Goodness-of-fit parameter for all reflections included in the refinement: 0.959
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No