Information card for entry 4304801

Structure parameters

• Formula: C97 H100 Cl2 Ge4 Ni6 S12
• Calculated formula: C97 H100 Cl2 Ge4 Ni6 S12
• Title of publication: Synthesis of Ge2NiS4 Clusters and the Thermal Transformation to a Ge4Ni6S12 Cluster
• Authors of publication: Tsuyoshi Matsumoto; Yosuke Matsui; Mikinao Ito; Kazuyuki Tatsumi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 1901 - 1903
• a: 22.913 ± 0.007 Å
• b: 16.604 ± 0.004 Å
• c: 27.451 ± 0.011 Å
• α: 90°
• β: 101.493 ± 0.01°
• γ: 90°
• Cell volume: 10234 ± 6 ų
• Cell temperature: 193.1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.1156
• Weighted residual factors for all reflections included in the refinement: 0.3044
• Goodness-of-fit parameter for all reflections included in the refinement: 1.257
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No