Information card for entry 4305301

Structure parameters

• Formula: C52 H90 F24 N12 Ni6 O25
• Calculated formula: C52 H90 F24 N12 Ni6 O25
• Title of publication: Extended Triple-Bridged Ni(II)- and Co(II)-Hydroxamate Trinuclear Complexes: Synthesis, Crystal Structures, and Magnetic Properties
• Authors of publication: Z. Tomkowicz; S. Ostrovsky; H. Müller-Bunz; A. J. Hussein Eltmimi; M. Rams; D. A. Brown; W. Haase
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 6956 - 6963
• a: 16.0444 ± 0.0015 Å
• b: 36.222 ± 0.003 Å
• c: 15.2264 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8849 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 41
• Hermann-Mauguin space group symbol: A b a 2
• Hall space group symbol: A 2 -2ab
• Residual factor for all reflections: 0.0395
• Residual factor for significantly intense reflections: 0.0354
• Weighted residual factors for significantly intense reflections: 0.0878
• Weighted residual factors for all reflections included in the refinement: 0.0911
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No