Information card for entry 4306077

Structure parameters

• Common name: [{(2,4,6-C3H7)(C6H2)}2PNH2]
• Formula: C30 H48 N P
• Calculated formula: C30 H48 N P
• Title of publication: Functionalization of Aminophosphanes: Synthesis and X-Ray Crystal Structure of Novel Dilithium and Trilithium Complexes Containing Silicon-Fused Heteronuclear SiN2PLi Five-Membered Rings
• Authors of publication: Anukul Jana; Gerald Schwab; Herbert W. Roesky; Dietmar Stalke
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 8990 - 8994
• a: 9.631 ± 0.003 Å
• b: 10.779 ± 0.003 Å
• c: 14.484 ± 0.005 Å
• α: 106.199 ± 0.003°
• β: 95.848 ± 0.004°
• γ: 98.495 ± 0.003°
• Cell volume: 1411.8 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0515
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.1232
• Weighted residual factors for all reflections included in the refinement: 0.1281
• Goodness-of-fit parameter for all reflections included in the refinement: 1.025
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No