Information card for entry 4306078

Structure parameters

• Common name: [Me2Si(NPtBu2)2Li2(THF)3]
• Formula: C30 H66 Li2 N2 O3 P2 Si
• Calculated formula: C30 H66 Li2 N2 O3 P2 Si
• Title of publication: Functionalization of Aminophosphanes: Synthesis and X-Ray Crystal Structure of Novel Dilithium and Trilithium Complexes Containing Silicon-Fused Heteronuclear SiN2PLi Five-Membered Rings
• Authors of publication: Anukul Jana; Gerald Schwab; Herbert W. Roesky; Dietmar Stalke
• Journal of publication: Inorganic Chemistry
• Year of publication: 2008
• Journal volume: 47
• Pages of publication: 8990 - 8994
• a: 11.7583 ± 0.0006 Å
• b: 18.0055 ± 0.0009 Å
• c: 19.3288 ± 0.001 Å
• α: 87.788 ± 0.001°
• β: 72.923 ± 0.001°
• γ: 73.467 ± 0.001°
• Cell volume: 3745.5 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0554
• Residual factor for significantly intense reflections: 0.0426
• Weighted residual factors for significantly intense reflections: 0.1127
• Weighted residual factors for all reflections included in the refinement: 0.1197
• Goodness-of-fit parameter for all reflections included in the refinement: 1.058
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No