Information card for entry 4307527

Structure parameters

• Common name: [(epppa)Zn](ClO4)2
• Formula: C21 H30 Cl2 N4 O9 S Zn
• Calculated formula: C21 H30 Cl2 N4 O9 S Zn
• Title of publication: Influence of the Chelate Ligand Structure on the Amide Methanolysis Reactivity of Mononuclear Zinc Complexes
• Authors of publication: Gajendrasingh K. Ingle; Magdalena M. Makowska-Grzyska; Ewa Szajna-Fuller; Indranil Sen; John C. Price; Atta M. Arif; Lisa M. Berreau
• Journal of publication: Inorganic Chemistry
• Year of publication: 2007
• Journal volume: 46
• Pages of publication: 1471 - 1480
• a: 9.4708 ± 0.0009 Å
• b: 12.1353 ± 0.0008 Å
• c: 12.129 ± 0.0011 Å
• α: 90°
• β: 100.544 ± 0.003°
• γ: 90°
• Cell volume: 1370.5 ± 0.2 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1277
• Residual factor for significantly intense reflections: 0.0767
• Weighted residual factors for significantly intense reflections: 0.1661
• Weighted residual factors for all reflections included in the refinement: 0.1949
• Goodness-of-fit parameter for all reflections included in the refinement: 1.04
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No