Crystallography Open Database

Information card for entry 4307528

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Coordinates	4307528.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H60 N8 O62 S2 W18
Calculated formula	C30.84 N8 O62 S2 W18
Title of publication	Synthesis and Voltammetry of [bmim]4[α-S2W18O62] and Related Compounds: Rapid Precipitation and Dissolution of Reduced Surface Films
Authors of publication	Andrew W. A. Mariotti; Jingli Xie; Brendan F. Abrahams; Alan M. Bond; Anthony G. Wedd
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Pages of publication	2530 - 2540
a	14.3737 ± 0.0009 Å
b	16.2349 ± 0.001 Å
c	19.1426 ± 0.0012 Å
α	88.632 ± 0.001°
β	81.764 ± 0.001°
γ	75.257 ± 0.001°
Cell volume	4275 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	130 ± 1 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1206
Residual factor for significantly intense reflections	0.1037
Weighted residual factors for significantly intense reflections	0.2583
Weighted residual factors for all reflections included in the refinement	0.2735
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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