Information card for entry 4312396

Structure parameters

• Formula: C42 H36 Cl2 N4 P4 Pd
• Calculated formula: C42 H36 Cl2 N4 P4 Pd
• Title of publication: Diphosphines Possessing Electronically Different Donor Groups: Synthesis and Coordination Chemistry of the Unsymmetrical Di(N-pyrrolyl)phosphino-Functionalized dppm Analogue Ph2PCH2P(NC4H4)2
• Authors of publication: Andrew D. Burrows; Mary F. Mahon; Steven P. Nolan; Maurizio Varrone
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7227 - 7238
• a: 9.382 ± 0.0002 Å
• b: 10.53 ± 0.0002 Å
• c: 22.689 ± 0.0004 Å
• α: 91.146 ± 0.001°
• β: 99.395 ± 0.001°
• γ: 109.799 ± 0.001°
• Cell volume: 2073.85 ± 0.07 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0649
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1004
• Weighted residual factors for all reflections included in the refinement: 0.1114
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No