Information card for entry 4312397

Structure parameters

• Formula: C42.25 H40 Cl2.5 N4 O2 P4 Pd2
• Calculated formula: C42.25 H40 Cl2.5 N4 P4 Pd2
• Title of publication: Diphosphines Possessing Electronically Different Donor Groups: Synthesis and Coordination Chemistry of the Unsymmetrical Di(N-pyrrolyl)phosphino-Functionalized dppm Analogue Ph2PCH2P(NC4H4)2
• Authors of publication: Andrew D. Burrows; Mary F. Mahon; Steven P. Nolan; Maurizio Varrone
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7227 - 7238
• a: 13.258 ± 0.0002 Å
• b: 15.83 ± 0.0002 Å
• c: 21.094 ± 0.0003 Å
• α: 90°
• β: 107.709 ± 0.0008°
• γ: 90°
• Cell volume: 4217.3 ± 0.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.072
• Residual factor for significantly intense reflections: 0.0474
• Weighted residual factors for significantly intense reflections: 0.1387
• Weighted residual factors for all reflections included in the refinement: 0.1653
• Goodness-of-fit parameter for all reflections included in the refinement: 0.826
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No