Information card for entry 4312620

Structure parameters

• Formula: C29 H28 Fe I N2 O P Zn
• Calculated formula: C29.152 H28.304 Fe I1.038 N2 O1.038 P Zn
• Title of publication: Synthesis and Structural Characterization of Double Metal Cyanides of Iron and Zinc: Catalyst Precursors for the Copolymerization of Carbon Dioxide and Epoxides
• Authors of publication: Donald J. Darensbourg; M. Jason Adams; Jason C. Yarbrough; Andrea L. Phelps
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7809 - 7818
• a: 10.936 ± 0.004 Å
• b: 15.982 ± 0.006 Å
• c: 16.338 ± 0.006 Å
• α: 90°
• β: 90.362 ± 0.008°
• γ: 90°
• Cell volume: 2855.5 ± 1.8 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.2795
• Residual factor for significantly intense reflections: 0.2084
• Weighted residual factors for significantly intense reflections: 0.5187
• Weighted residual factors for all reflections included in the refinement: 0.5354
• Goodness-of-fit parameter for all reflections included in the refinement: 1.641
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No