Information card for entry 4312621

Structure parameters

• Formula: C125 H105 Ag2 Fe4 I4 N13 P4 Zn3
• Calculated formula: C69.46 H58.3 Ag0.557 Fe1.99 I1.433 N8 P2 Zn1.5
• Title of publication: Synthesis and Structural Characterization of Double Metal Cyanides of Iron and Zinc: Catalyst Precursors for the Copolymerization of Carbon Dioxide and Epoxides
• Authors of publication: Donald J. Darensbourg; M. Jason Adams; Jason C. Yarbrough; Andrea L. Phelps
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7809 - 7818
• a: 14.24 ± 0.004 Å
• b: 16.089 ± 0.005 Å
• c: 17.644 ± 0.005 Å
• α: 63.302 ± 0.006°
• β: 69.002 ± 0.006°
• γ: 79.22 ± 0.006°
• Cell volume: 3369.9 ± 1.7 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.2637
• Residual factor for significantly intense reflections: 0.1902
• Weighted residual factors for significantly intense reflections: 0.4874
• Weighted residual factors for all reflections included in the refinement: 0.5102
• Goodness-of-fit parameter for all reflections included in the refinement: 1.468
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No