Information card for entry 4312622

Structure parameters

• Formula: C35 H30 Ag Fe I2 N4 P Zn
• Calculated formula: C35 H30 Ag Fe I2 N4 P Zn
• Title of publication: Synthesis and Structural Characterization of Double Metal Cyanides of Iron and Zinc: Catalyst Precursors for the Copolymerization of Carbon Dioxide and Epoxides
• Authors of publication: Donald J. Darensbourg; M. Jason Adams; Jason C. Yarbrough; Andrea L. Phelps
• Journal of publication: Inorganic Chemistry
• Year of publication: 2003
• Journal volume: 42
• Pages of publication: 7809 - 7818
• a: 13.415 ± 0.004 Å
• b: 11.005 ± 0.003 Å
• c: 25.062 ± 0.007 Å
• α: 90°
• β: 104.232 ± 0.005°
• γ: 90°
• Cell volume: 3586.4 ± 1.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0229
• Weighted residual factors for significantly intense reflections: 0.0389
• Weighted residual factors for all reflections included in the refinement: 0.0407
• Goodness-of-fit parameter for all reflections included in the refinement: 0.824
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No