Information card for entry 4316449

Structure parameters

• Formula: C22 H34 Cl2 Cu3 N10 O2
• Calculated formula: C22 H34 Cl2 Cu3 N10 O2
• Title of publication: Use of a Reduced Schiff-Base Ligand to Prepare Novel Chloro-Bridged Chains of Rare Cu(II) Trinuclear Complexes with Mixed Azido/Oxo and Chloro/Oxo Bridges
• Authors of publication: Apurba Biswas; Michael G. B. Drew; Carlos J. Gómez-García; Ashutosh Ghosh
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 8155 - 8163
• a: 11.5818 ± 0.0006 Å
• b: 16.2364 ± 0.0009 Å
• c: 16.2417 ± 0.0009 Å
• α: 90°
• β: 110.392 ± 0.006°
• γ: 90°
• Cell volume: 2862.8 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0888
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.076
• Weighted residual factors for all reflections included in the refinement: 0.0818
• Goodness-of-fit parameter for all reflections included in the refinement: 0.832
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No