Information card for entry 4316450

Structure parameters

• Formula: C22.46 H35.84 Cl4 Cu3 N4 O2.46
• Calculated formula: C22.457 H35.828 Cl4 Cu3 N4 O2.457
• Title of publication: Use of a Reduced Schiff-Base Ligand to Prepare Novel Chloro-Bridged Chains of Rare Cu(II) Trinuclear Complexes with Mixed Azido/Oxo and Chloro/Oxo Bridges
• Authors of publication: Apurba Biswas; Michael G. B. Drew; Carlos J. Gómez-García; Ashutosh Ghosh
• Journal of publication: Inorganic Chemistry
• Year of publication: 2010
• Journal volume: 49
• Pages of publication: 8155 - 8163
• a: 11.4006 ± 0.0006 Å
• b: 17.475 ± 0.0006 Å
• c: 15.075 ± 0.0007 Å
• α: 90°
• β: 104.487 ± 0.005°
• γ: 90°
• Cell volume: 2907.8 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1352
• Residual factor for significantly intense reflections: 0.0939
• Weighted residual factors for significantly intense reflections: 0.1821
• Weighted residual factors for all reflections included in the refinement: 0.1913
• Goodness-of-fit parameter for all reflections included in the refinement: 1.246
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No