Information card for entry 4318042

Structure parameters

• Chemical name: Catena-{tris[tetrakis(trifluoroacetato)dirhodium(II,II)]-tris (4'-pyridyl)methanol-(η1-benzene)}, benzene solvate
• Formula: C49 H22 F36 N3 O25 Rh6
• Calculated formula: C49 H19 F36 N3 O25 Rh6
• Title of publication: Supramolecular Assemblies of Dimetal Complexes with Polydentate N-Donor Ligands: From a Discrete Pyramid to a 3D Channel Network
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Marina A. Petrukhina; Marion Schmitz; Peter J. Stang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 2903 - 2908
• a: 23.175 ± 0.002 Å
• b: 16.1746 ± 0.0007 Å
• c: 23.782 ± 0.004 Å
• α: 90°
• β: 93.101 ± 0.007°
• γ: 90°
• Cell volume: 8901.5 ± 1.7 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.098
• Residual factor for significantly intense reflections: 0.08
• Weighted residual factors for significantly intense reflections: 0.2093
• Weighted residual factors for all reflections included in the refinement: 0.2309
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No