Information card for entry 4318043

Structure parameters

• Chemical name: {Tris[tetrakis(trifluoroacetato)dirhodium(II,II)]-tris(4'-pyridyl) methylsilane-tris(η1-benzene)}, benzene solvate
• Formula: C64 H39 F36 N3 O24 Rh6 Si
• Calculated formula: C63.97 H35.97 F36 N3 O24 Rh6 Si
• Title of publication: Supramolecular Assemblies of Dimetal Complexes with Polydentate N-Donor Ligands: From a Discrete Pyramid to a 3D Channel Network
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Marina A. Petrukhina; Marion Schmitz; Peter J. Stang
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 2903 - 2908
• a: 25.16 ± 0.002 Å
• b: 25.16 ± 0.002 Å
• c: 23.382 ± 0.005 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 12818 ± 3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0551
• Residual factor for significantly intense reflections: 0.0475
• Weighted residual factors for all reflections: 0.124
• Weighted residual factors for significantly intense reflections: 0.1132
• Goodness-of-fit parameter for all reflections: 1.051
• Goodness-of-fit parameter for significantly intense reflections: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No