Information card for entry 4319014

Structure parameters

• Formula: C22 H39 Li2 N2 O2 P Se
• Calculated formula: C21.98 H39 Li2 N2 O2 P Se
• Title of publication: Synthesis and X-ray Structures of Dilithium Complexes of the Phosphonate Anions [PhP(E)(NtBu)2]2- (E = O, S, Se, Te) and Dimethylaluminum Derivatives of [PhP(E)(NtBu)(NHtBu)]- (E = S, Se)
• Authors of publication: Glen G. Briand; Tristram Chivers; Mark Krahn; Masood Parvez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 6808 - 6815
• a: 9.413 ± 0.0001 Å
• b: 10.2438 ± 0.0002 Å
• c: 15.1293 ± 0.0002 Å
• α: 89.009 ± 0.001°
• β: 73.194 ± 0.001°
• γ: 66.39 ± 0.001°
• Cell volume: 1271.54 ± 0.04 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0392
• Residual factor for significantly intense reflections: 0.0373
• Weighted residual factors for significantly intense reflections: 0.0958
• Weighted residual factors for all reflections included in the refinement: 0.0978
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No