Information card for entry 4319015

Structure parameters

• Formula: C22 H39 Li2 N2 O2 P Te
• Calculated formula: C22 H39 Li2 N2 O2 P Te
• Title of publication: Synthesis and X-ray Structures of Dilithium Complexes of the Phosphonate Anions [PhP(E)(NtBu)2]2- (E = O, S, Se, Te) and Dimethylaluminum Derivatives of [PhP(E)(NtBu)(NHtBu)]- (E = S, Se)
• Authors of publication: Glen G. Briand; Tristram Chivers; Mark Krahn; Masood Parvez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 6808 - 6815
• a: 9.2017 ± 0.0002 Å
• b: 10.1328 ± 0.0002 Å
• c: 15.8982 ± 0.0004 Å
• α: 94.6527 ± 0.0007°
• β: 104.786 ± 0.0008°
• γ: 110.95 ± 0.0009°
• Cell volume: 1313.89 ± 0.05 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.056
• Residual factor for significantly intense reflections: 0.0493
• Weighted residual factors for significantly intense reflections: 0.147
• Weighted residual factors for all reflections included in the refinement: 0.1504
• Goodness-of-fit parameter for all reflections included in the refinement: 1.186
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No