Information card for entry 4319980

Structure parameters

• Formula: C84.7 H45.4 B2 Cl1.4 F48 N12 Pb
• Calculated formula: C84.7 H45.4 B2 Cl1.4 F48 N12 Pb
• Title of publication: Control of the Stereochemical Impact of the Lone Pair in Lead(II) Tris(pyrazolyl)methane Complexes. Improved Preparation of Na{B[3,5-(CF3)2C6H3]4}
• Authors of publication: Daniel L. Reger; Terri D. Wright; Christine A. Little; Jaydeep J. S. Lamba; Mark D. Smith
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 3810 - 3814
• a: 13.0133 ± 0.0006 Å
• b: 17.221 ± 0.0007 Å
• c: 24.7634 ± 0.0011 Å
• α: 71.73 ± 0.001°
• β: 82.363 ± 0.001°
• γ: 70.512 ± 0.001°
• Cell volume: 4965.4 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0871
• Residual factor for significantly intense reflections: 0.0611
• Weighted residual factors for significantly intense reflections: 0.1631
• Weighted residual factors for all reflections included in the refinement: 0.1755
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No