Information card for entry 4319981

Structure parameters

• Formula: C98 H72 B2 Cl4 F48 N12 Pb
• Calculated formula: C98 H72 B2 Cl4 F48 N12 Pb
• Title of publication: Control of the Stereochemical Impact of the Lone Pair in Lead(II) Tris(pyrazolyl)methane Complexes. Improved Preparation of Na{B[3,5-(CF3)2C6H3]4}
• Authors of publication: Daniel L. Reger; Terri D. Wright; Christine A. Little; Jaydeep J. S. Lamba; Mark D. Smith
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 3810 - 3814
• a: 12.756 ± 0.004 Å
• b: 13.469 ± 0.004 Å
• c: 17.16 ± 0.005 Å
• α: 82.454 ± 0.007°
• β: 89.904 ± 0.008°
• γ: 72.995 ± 0.007°
• Cell volume: 2792.9 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1401
• Residual factor for significantly intense reflections: 0.0661
• Weighted residual factors for significantly intense reflections: 0.1495
• Weighted residual factors for all reflections included in the refinement: 0.1699
• Goodness-of-fit parameter for all reflections included in the refinement: 1.013
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No