Information card for entry 4320958

Structure parameters

• Chemical name: [{1,1,1-tris(diphenylphosphinomethyl)ethane cobalt}(=B5,h3:1-cyclotriphosphorus) (rhenium pentacarbonyl)]tetrafluoroborate
• Formula: C53 H47 B Co F4 O5 P6 Re
• Calculated formula: C52 H45 B Co F4 O5 P6 Re
• Title of publication: Cyclotriphosphorus Complexes: Solid-State Structures and Dynamic Behavior of Monoadducts with Carbonyl Fragments
• Authors of publication: Massimo Di Vaira; Markus P. Ehses; Piero Stoppioni; Maurizio Peruzzini
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2199 - 2205
• a: 14.754 ± 0.002 Å
• b: 24.886 ± 0.004 Å
• c: 15.182 ± 0.002 Å
• α: 90°
• β: 103.38 ± 0.01°
• γ: 90°
• Cell volume: 5423 ± 1.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0704
• Residual factor for significantly intense reflections: 0.0529
• Weighted residual factors for all reflections: 0.1284
• Weighted residual factors for significantly intense reflections: 0.1228
• Goodness-of-fit parameter for all reflections: 0.9
• Goodness-of-fit parameter for significantly intense reflections: 1.084
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No