Crystallography Open Database

Information card for entry 4321016

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Coordinates	4321016.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C38 H57 Cl6 N2 O2 Rh
Calculated formula	C38 H57 Cl6 N2 O2 Rh
Title of publication	Synthesis and Characterization of Rhodium(III) Dichloro Complexes with Unsymmetrically Bound Salen-Type Ligands
Authors of publication	Renee A. Stinziano-Eveland; SonBinh T. Nguyen; Louise M. Liable-Sands; Arnold L. Rheingold
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	2452 - 2455
a	12.5463 ± 0.0003 Å
b	12.4447 ± 0.0003 Å
c	28.2073 ± 0.0007 Å
α	90°
β	96.4862 ± 0.0009°
γ	90°
Cell volume	4375.95 ± 0.18 Å³
Cell temperature	198 ± 2 K
Ambient diffraction temperature	198 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0956
Residual factor for significantly intense reflections	0.0587
Weighted residual factors for all reflections	0.1377
Weighted residual factors for significantly intense reflections	0.1213
Goodness-of-fit parameter for all reflections	1.29
Goodness-of-fit parameter for significantly intense reflections	1.403
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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