Information card for entry 4321017

Structure parameters

• Formula: F8 O2 Sb Tc
• Calculated formula: F8 O2 Sb Tc
• Title of publication: Fluoride Ion Donor Properties of TcO2F3 and ReO2F3: X-ray Crystal Structures of MO2F3.SbF5 (M = Tc, Re) and TcO2F3.XeO2F2 and Raman and NMR Spectroscopic Characterization of MO2F3.PnF5 (Pn = As, Sb), [ReO2F2(CH3CN)2][SbF6], and [Re2O4F5][Sb2F11]
• Authors of publication: Nicolas LeBlond; David A. Dixon; Gary J. Schrobilgen
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2473 - 2487
• a: 7.3655 ± 0.0015 Å
• b: 10.441 ± 0.002 Å
• c: 9.398 ± 0.002 Å
• α: 90°
• β: 93.32 ± 0.03°
• γ: 90°
• Cell volume: 721.5 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0676
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for all reflections: 0.1112
• Weighted residual factors for significantly intense reflections: 0.1047
• Goodness-of-fit parameter for all reflections: 0.911
• Goodness-of-fit parameter for significantly intense reflections: 1.041
• Diffraction radiation wavelength: 0.56086 Å
• Diffraction radiation type: AgKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No