Information card for entry 4321178

Structure parameters

• Formula: C64 H80 B N4 O8 P4 Re
• Calculated formula: C64.364 H78.22 B0.911 Cl0.089 N3.822 O8 P4 Re
• Title of publication: Diazo Complexes of Rhenium: Preparations and Crystal Structures of the Bis(dinitrogen), [Re(N2)2{PPh(OEt)2}4][BPh4] and Methyldiazenido [ReCl(CH3N2)(CH3NHNH2){PPh(OEt)2}3][BPh4] Derivatives
• Authors of publication: Gabriele Albertin; Stefano Antoniutti; Alessia Bacchi; Emilio Bordignon; Francesca Miani; Giancarlo Pelizzi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 3283 - 3293
• a: 23.008 ± 0.005 Å
• b: 23.367 ± 0.005 Å
• c: 12.863 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6916 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 54
• Hermann-Mauguin space group symbol: P b a a
• Hall space group symbol: -P 2a 2b
• Residual factor for all reflections: 0.1629
• Residual factor for significantly intense reflections: 0.0463
• Weighted residual factors for significantly intense reflections: 0.1047
• Weighted residual factors for all reflections included in the refinement: 0.1367
• Goodness-of-fit parameter for all reflections included in the refinement: 0.92
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No