Information card for entry 4321179

Structure parameters

• Formula: C56 H74 B Cl N4 O6 P3 Re
• Calculated formula: C56 H74 B Cl N4 O6 P3 Re
• Title of publication: Diazo Complexes of Rhenium: Preparations and Crystal Structures of the Bis(dinitrogen), [Re(N2)2{PPh(OEt)2}4][BPh4] and Methyldiazenido [ReCl(CH3N2)(CH3NHNH2){PPh(OEt)2}3][BPh4] Derivatives
• Authors of publication: Gabriele Albertin; Stefano Antoniutti; Alessia Bacchi; Emilio Bordignon; Francesca Miani; Giancarlo Pelizzi
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 3283 - 3293
• a: 15.396 ± 0.005 Å
• b: 16.986 ± 0.005 Å
• c: 11.56 ± 0.005 Å
• α: 93.959 ± 0.005°
• β: 93.988 ± 0.005°
• γ: 93.087 ± 0.005°
• Cell volume: 3003.4 ± 1.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0623
• Residual factor for significantly intense reflections: 0.034
• Weighted residual factors for significantly intense reflections: 0.0661
• Weighted residual factors for all reflections included in the refinement: 0.0725
• Goodness-of-fit parameter for all reflections included in the refinement: 0.889
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No