Information card for entry 4321451

Structure parameters

• Formula: C36 H70 O5 P2 Si4 Sm
• Calculated formula: C36 H70 O5 P2 Si4 Sm
• Title of publication: Synthesis and Structural Characterization of Sm(II) and Yb(II) Complexes Containing Sterically Demanding, Chelating Secondary Phosphide Ligands
• Authors of publication: Keith Izod; Paul O'Shaughnessy; Joanne M. Sheffield; William Clegg; Stephen T. Liddle
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 4741 - 4748
• a: 11.0625 ± 0.0009 Å
• b: 15.9246 ± 0.0012 Å
• c: 17.2104 ± 0.0014 Å
• α: 72.327 ± 0.002°
• β: 83.934 ± 0.002°
• γ: 79.556 ± 0.002°
• Cell volume: 2836.8 ± 0.4 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0915
• Residual factor for significantly intense reflections: 0.0648
• Weighted residual factors for significantly intense reflections: 0.1696
• Weighted residual factors for all reflections included in the refinement: 0.189
• Goodness-of-fit parameter for all reflections included in the refinement: 1.073
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No