Information card for entry 4321452

Structure parameters

• Formula: C38 H76 O5 P2 Si4 Sm
• Calculated formula: C38 H76 O5 P2 Si4 Sm
• Title of publication: Synthesis and Structural Characterization of Sm(II) and Yb(II) Complexes Containing Sterically Demanding, Chelating Secondary Phosphide Ligands
• Authors of publication: Keith Izod; Paul O'Shaughnessy; Joanne M. Sheffield; William Clegg; Stephen T. Liddle
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 4741 - 4748
• a: 13.176 ± 0.004 Å
• b: 13.08 ± 0.004 Å
• c: 14.546 ± 0.004 Å
• α: 90°
• β: 95.363 ± 0.006°
• γ: 90°
• Cell volume: 2495.9 ± 1.3 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1251
• Residual factor for significantly intense reflections: 0.1015
• Weighted residual factors for significantly intense reflections: 0.2418
• Weighted residual factors for all reflections included in the refinement: 0.2533
• Goodness-of-fit parameter for all reflections included in the refinement: 1.033
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No