Crystallography Open Database

Information card for entry 4321488

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Coordinates	4321488.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H86 N4 Na2 P4 Si4
Calculated formula	C69 H78 N4 Na2 P4 Si4
Title of publication	Dimeric Bridged and Chelated Alkali Metal (Li and Na) Bis(iminophosphorano)methanide Complexes with Contrasting Structures
Authors of publication	Ruppa P. Kamalesh Babu; Kasani Aparna; Robert McDonald; Ronald G. Cavell
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	4981 - 4984
a	12.3907 ± 0.001 Å
b	14.5179 ± 0.0011 Å
c	21.3739 ± 0.0014 Å
α	76.1521 ± 0.0015°
β	86.5411 ± 0.0016°
γ	73.2969 ± 0.0013°
Cell volume	3575.5 ± 0.5 Å³
Cell temperature	193 ± 2 K
Ambient diffraction temperature	193 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1178
Residual factor for significantly intense reflections	0.0656
Weighted residual factors for significantly intense reflections	0.1654
Weighted residual factors for all reflections included in the refinement	0.1861
Goodness-of-fit parameter for all reflections included in the refinement	0.948
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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