Information card for entry 4321489

Structure parameters

• Formula: C69 H86 Li2 N4 P4 Si4
• Calculated formula: C69 H78 Li2 N4 P4 Si4
• Title of publication: Dimeric Bridged and Chelated Alkali Metal (Li and Na) Bis(iminophosphorano)methanide Complexes with Contrasting Structures
• Authors of publication: Ruppa P. Kamalesh Babu; Kasani Aparna; Robert McDonald; Ronald G. Cavell
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 4981 - 4984
• a: 13.5173 ± 0.0012 Å
• b: 21.335 ± 0.002 Å
• c: 24.581 ± 0.002 Å
• α: 90°
• β: 91.086 ± 0.002°
• γ: 90°
• Cell volume: 7087.7 ± 1.1 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1407
• Residual factor for significantly intense reflections: 0.0807
• Weighted residual factors for significantly intense reflections: 0.2042
• Weighted residual factors for all reflections included in the refinement: 0.2281
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No