Information card for entry 4321492

Structure parameters

• Formula: C48 H40 Mn2 Mo N16 O4
• Calculated formula: C48 H32 Mn2 Mo N16 O4
• Title of publication: X-ray Evidence of CN Bridging in Bimetallic Complexes Based on [M(CN)8]4- (M = Mo, W). The Crystal Structure of {[Mn(bpy)2]2(μ-NC)2[Mo(CN)6]2(μ-CN)2[Mn(bpy)2]2}.8H2O
• Authors of publication: Barbara Sieklucka; Janusz Szklarzewicz; Terence J. Kemp; William Errington
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 5156 - 5158
• a: 13.9804 ± 0.001 Å
• b: 22.8924 ± 0.0012 Å
• c: 15.5757 ± 0.0012 Å
• α: 90°
• β: 91.71 ± 0.003°
• γ: 90°
• Cell volume: 4982.7 ± 0.6 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1257
• Residual factor for significantly intense reflections: 0.0644
• Weighted residual factors for significantly intense reflections: 0.1333
• Weighted residual factors for all reflections included in the refinement: 0.1635
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No