Information card for entry 4321493

Structure parameters

• Formula: C24 H60 Cl Fe Li N2 O3 Si4
• Calculated formula: C24 H60 Cl Fe Li N2 O3 Si4
• SMILES: [Fe]([Cl][Li]([O]1CCCC1)([O]1CCCC1)[O]1CCCC1)(N([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C
• Title of publication: (THF)3LiCl as a Ligand for Low-Coordinate Fe(II): Crystal Structure of [(Me~3~Si)~2~N]~2~Fe(μ-Cl)Li(THF)~3~
• Authors of publication: Ulrich Siemeling; Udo Vorfeld; Beate Neumann; Hans-Georg Stammler
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 5159 - 5160
• a: 12.122 ± 0.006 Å
• b: 12.627 ± 0.005 Å
• c: 14.352 ± 0.006 Å
• α: 82.75 ± 0.03°
• β: 85.38 ± 0.04°
• γ: 61.57 ± 0.03°
• Cell volume: 1915.9 ± 1.6 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1692
• Residual factor for significantly intense reflections: 0.0987
• Weighted residual factors for significantly intense reflections: 0.2481
• Weighted residual factors for all reflections included in the refinement: 0.3006
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No