Information card for entry 4321496

Structure parameters

• Formula: C124 H148 Mo2 N4 O12
• Calculated formula: C124 H148 Mo2 N4 O12
• Title of publication: Group 6 Metallocalixarenes Bearing "Hydrazido(2-)" Groups
• Authors of publication: Carl Redshaw; Mark R. J. Elsegood
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 5164 - 5168
• a: 16.0888 ± 0.0011 Å
• b: 17.7004 ± 0.0012 Å
• c: 19.4921 ± 0.0014 Å
• α: 90°
• β: 91.078 ± 0.002°
• γ: 90°
• Cell volume: 5549.9 ± 0.7 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0845
• Residual factor for significantly intense reflections: 0.0595
• Weighted residual factors for significantly intense reflections: 0.1362
• Weighted residual factors for all reflections included in the refinement: 0.152
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No