Information card for entry 4321495

Structure parameters

• Formula: C120.5 H138 Cl5 N7 O8 W2
• Calculated formula: C120.5 H138 Cl5 N7 O8 W2
• Title of publication: Group 6 Metallocalixarenes Bearing "Hydrazido(2-)" Groups
• Authors of publication: Carl Redshaw; Mark R. J. Elsegood
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 5164 - 5168
• a: 16.7386 ± 0.0014 Å
• b: 18.809 ± 0.002 Å
• c: 20.0969 ± 0.0017 Å
• α: 94.791 ± 0.006°
• β: 108.422 ± 0.005°
• γ: 99.972 ± 0.008°
• Cell volume: 5847.2 ± 1 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0718
• Residual factor for significantly intense reflections: 0.0554
• Weighted residual factors for significantly intense reflections: 0.1444
• Weighted residual factors for all reflections included in the refinement: 0.1511
• Goodness-of-fit parameter for all reflections included in the refinement: 0.986
• Diffraction radiation wavelength: 0.6875 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No