Information card for entry 4321774

Structure parameters

• Chemical name: Bis(μ2-bis(diphenylphosphino)methane-P,P')-tetrachloro- -di-molybdenum(II), dichloromethane solvate
• Formula: C52 H48 Cl8 Mo2 P4
• Calculated formula: C52 H44 Cl8 Mo2 P4
• Title of publication: Mixed Chloride/Amine Complexes of Dimolybdenum(II,II). 2. Reactions of Mo2Cl4(NHEt2)4 with Monodentate and Bidentate Phosphines. New Type of Compounds Mo2Cl4(diphosphine)4
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Santiago Herrero
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 490 - 495
• a: 18.03 ± 0.001 Å
• b: 14.5108 ± 0.0007 Å
• c: 23.221 ± 0.001 Å
• α: 90°
• β: 112.778 ± 0.004°
• γ: 90°
• Cell volume: 5601.5 ± 0.5 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0624
• Residual factor for significantly intense reflections: 0.058
• Weighted residual factors for all reflections: 0.1657
• Weighted residual factors for significantly intense reflections: 0.1587
• Goodness-of-fit parameter for all reflections: 1.102
• Goodness-of-fit parameter for significantly intense reflections: 1.107
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No