Information card for entry 4321773

Structure parameters

• Chemical name: Bis(μ2-bis(dimethylphosphino)methane-P,P')-tetrachloro- -di-molybdenum(II), hexane solvate
• Formula: C13 H35 Cl4 Mo2 P4
• Calculated formula: C13 H35 Cl4 Mo2 P4
• Title of publication: Mixed Chloride/Amine Complexes of Dimolybdenum(II,II). 2. Reactions of Mo2Cl4(NHEt2)4 with Monodentate and Bidentate Phosphines. New Type of Compounds Mo2Cl4(diphosphine)4
• Authors of publication: F. Albert Cotton; Evgeny V. Dikarev; Santiago Herrero
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 490 - 495
• a: 12.699 ± 0.002 Å
• b: 12.699 ± 0.002 Å
• c: 16.015 ± 0.004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2582.7 ± 0.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 82
• Hermann-Mauguin space group symbol: I -4
• Hall space group symbol: I -4
• Residual factor for all reflections: 0.0496
• Residual factor for significantly intense reflections: 0.0308
• Weighted residual factors for all reflections: 0.0866
• Weighted residual factors for significantly intense reflections: 0.0785
• Goodness-of-fit parameter for all reflections: 1.053
• Goodness-of-fit parameter for significantly intense reflections: 1.102
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No