Information card for entry 4322770

Structure parameters

• Formula: C12 H27 Li3 N3 Sb
• Calculated formula: C12 H27 Li3 N3 Sb
• Title of publication: Heterobimetallic (Imido)antimony/Lithium Cages Containing [Sb(NR)3]3- Trianions
• Authors of publication: Michael A. Beswick; Nick Choi; Christopher N. Harmer; Alexander D. Hopkins; Mary McPartlin; Michael A. Paver; Paul R. Raithby; Alexander Steiner; Mustafa Tombul; Dominic S. Wright
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 2177 - 2182
• a: 9.9942 ± 0.0012 Å
• b: 17.421 ± 0.002 Å
• c: 10.68 ± 0.002 Å
• α: 90°
• β: 111.331 ± 0.012°
• γ: 90°
• Cell volume: 1732.1 ± 0.5 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0982
• Residual factor for significantly intense reflections: 0.0491
• Weighted residual factors for all reflections: 0.1494
• Weighted residual factors for significantly intense reflections: 0.1057
• Goodness-of-fit parameter for all reflections: 1.129
• Goodness-of-fit parameter for significantly intense reflections: 1.208
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No