Information card for entry 4322771

Structure parameters

• Formula: C70 H86 Li6 N6 O14 Sb2
• Calculated formula: C70 H86 Li6 N6 O14 Sb2
• Title of publication: Heterobimetallic (Imido)antimony/Lithium Cages Containing [Sb(NR)3]3- Trianions
• Authors of publication: Michael A. Beswick; Nick Choi; Christopher N. Harmer; Alexander D. Hopkins; Mary McPartlin; Michael A. Paver; Paul R. Raithby; Alexander Steiner; Mustafa Tombul; Dominic S. Wright
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 2177 - 2182
• a: 10.435 ± 0.004 Å
• b: 12.654 ± 0.005 Å
• c: 14.278 ± 0.006 Å
• α: 75.31 ± 0.04°
• β: 79.02 ± 0.03°
• γ: 84.33 ± 0.04°
• Cell volume: 1787.8 ± 1.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0306
• Residual factor for significantly intense reflections: 0.0292
• Weighted residual factors for all reflections: 0.0767
• Weighted residual factors for significantly intense reflections: 0.073
• Goodness-of-fit parameter for all reflections: 1.1
• Goodness-of-fit parameter for significantly intense reflections: 1.104
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No