Information card for entry 4322863

Structure parameters

• Common name: {[(BispicMe2en)Fe]2(OH)(mu-O)(H2O),(ClO4)3,(H2O)
• Formula: C32 H49 Cl3 Fe2 N8 O16
• Calculated formula: C32 H48 Cl3 Fe2 N8 O16
• Title of publication: Synthesis, Structure, and Characterization of the New [L(OH)Fe(μ-O)Fe(OH2)L]3+ Complex (L = N,N'-Dimethyl-N,N'-bis(2-pyridylmethyl)ethane-1,2-diamine). Detection of an Equilibrium with the Protonated Diamond Form [LFe(μ-O)(μ-OH)FeL]3+ in Acetonitrile
• Authors of publication: Sandrine Poussereau; Geneviève Blondin; Michèle Cesario; Jean Guilhem; Geneviève Chottard; Florence Gonnet; Jean-Jacques Girerd
• Journal of publication: Inorganic Chemistry
• Year of publication: 1998
• Journal volume: 37
• Pages of publication: 3127 - 3132
• a: 13.283 ± 0.005 Å
• b: 16.05 ± 0.009 Å
• c: 20.996 ± 0.01 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4476 ± 4 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 6
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.1375
• Residual factor for significantly intense reflections: 0.0566
• Weighted residual factors for all reflections: 0.1842
• Weighted residual factors for significantly intense reflections: 0.1414
• Goodness-of-fit parameter for all reflections: 1.008
• Goodness-of-fit parameter for significantly intense reflections: 1.104
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No