Information card for entry 4323304

Structure parameters

• Formula: C18 H40 B O2 P4 Rh
• Calculated formula: C18 H40 B O2 P4 Rh
• SMILES: [Rh](B1Oc2c(O1)cccc2)([P](C)(C)C)([P](C)(C)C)([P](C)(C)C)[P](C)(C)C
• Title of publication: Synthesis and Characterization of Rhodium(I) Boryl and Rhodium(III) Tris(Boryl) Compounds: Molecular Structures of [(PMe3)4Rh(B(cat))] andfac-[(PMe3)3Rh(B(cat))3] (cat = 1,2-O2C6H4)
• Authors of publication: Chaoyang Dai; Graham Stringer; Todd B. Marder; Andrew J. Scott; William Clegg; Nicholas C. Norman
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 272 - 273
• a: 16.7763 ± 0.0012 Å
• b: 9.8236 ± 0.0007 Å
• c: 16.3714 ± 0.0012 Å
• α: 90°
• β: 103.728 ± 0.002°
• γ: 90°
• Cell volume: 2621 ± 0.3 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0321
• Residual factor for significantly intense reflections: 0.0278
• Weighted residual factors for all reflections: 0.0746
• Weighted residual factors for significantly intense reflections: 0.0694
• Goodness-of-fit parameter for all reflections: 1.161
• Goodness-of-fit parameter for significantly intense reflections: 1.144
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No