Information card for entry 4323305

Structure parameters

• Formula: C30.5 H43 B3 O6 P3 Rh
• Calculated formula: C30.5 H39 B3 O6 P3 Rh
• Title of publication: Synthesis and Characterization of Rhodium(I) Boryl and Rhodium(III) Tris(Boryl) Compounds: Molecular Structures of [(PMe3)4Rh(B(cat))] andfac-[(PMe3)3Rh(B(cat))3] (cat = 1,2-O2C6H4)
• Authors of publication: Chaoyang Dai; Graham Stringer; Todd B. Marder; Andrew J. Scott; William Clegg; Nicholas C. Norman
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 272 - 273
• a: 9.4861 ± 0.0009 Å
• b: 11.5356 ± 0.0011 Å
• c: 17.8907 ± 0.0018 Å
• α: 73.055 ± 0.003°
• β: 83.211 ± 0.002°
• γ: 68.39 ± 0.002°
• Cell volume: 1741 ± 0.3 ų
• Cell temperature: 160 ± 2 K
• Ambient diffraction temperature: 160 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0386
• Residual factor for significantly intense reflections: 0.0375
• Weighted residual factors for all reflections: 0.1023
• Weighted residual factors for significantly intense reflections: 0.1005
• Goodness-of-fit parameter for all reflections: 1.05
• Goodness-of-fit parameter for significantly intense reflections: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No