Information card for entry 4323508

Structure parameters

• Formula: C39 H34 Cl6 P2 Pd
• Calculated formula: C41 H32 Cl10 P2 Pd
• Title of publication: A Bidentate Bisphosphine Functioning in Intramolecular Aliphatic Metalation and as an NMR Spectroscopic Probe for the Metal Coordination Environment
• Authors of publication: William Lesueur; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli
• Journal of publication: Inorganic Chemistry
• Year of publication: 1997
• Journal volume: 36
• Pages of publication: 3354 - 3362
• a: 11.987 ± 0.001 Å
• b: 15.99 ± 0.002 Å
• c: 10.872 ± 0.001 Å
• α: 91.42 ± 0.01°
• β: 111.01 ± 0.02°
• γ: 99.86 ± 0.02°
• Cell volume: 1908.2 ± 0.5 ų
• Cell temperature: 25 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0537
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for all reflections: 0.1519
• Weighted residual factors for significantly intense reflections: 0.1427
• Goodness-of-fit parameter for all reflections: 1.102
• Goodness-of-fit parameter for significantly intense reflections: 1.034
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No