Crystallography Open Database

Information card for entry 4323509

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Coordinates	4323509.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C64 H54 P3 Pd
Calculated formula	C70 H48 P3 Pd
Title of publication	A Bidentate Bisphosphine Functioning in Intramolecular Aliphatic Metalation and as an NMR Spectroscopic Probe for the Metal Coordination Environment
Authors of publication	William Lesueur; Euro Solari; Carlo Floriani; Angiola Chiesi-Villa; Corrado Rizzoli
Journal of publication	Inorganic Chemistry
Year of publication	1997
Journal volume	36
Pages of publication	3354 - 3362
a	39.071 ± 0.005 Å
b	13.657 ± 0.004 Å
c	19.848 ± 0.005 Å
α	90 ± 0°
β	92.45 ± 0.02°
γ	90 ± 0°
Cell volume	10581 ± 4 Å³
Cell temperature	25 K
Ambient diffraction temperature	295 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.2222
Residual factor for significantly intense reflections	0.047
Weighted residual factors for all reflections	0.1684
Weighted residual factors for significantly intense reflections	0.1032
Goodness-of-fit parameter for all reflections	0.828
Goodness-of-fit parameter for significantly intense reflections	1.161
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKa
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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